Guidance document on analytical quality control and validation procedures for pesticide European Union (2014). May 10, 2015 · Document SANCO/12571/2013 on Analytical Quality Control and Validation Procedures for Pesticide Residues Analysis in Food and Feed Antonio Valverde – LAPRW 2015, Santiago de Chile (May 2015) Guidelines for residue data under Regulation 1107/2009 (or former Directive 91/414/EEC) and Regulation EC 396/2005 No category sanco/12571/2013 - EURL EUROPEAN COMMISSION HEALTH & CONSUMER PROTECTION DIRECTORATE-GENERAL Safety of the food chain Chemicals, contaminants, pesticides SANCO/12571/2013 19 November 2013 rev. Guidance_Sanco_2013_12571-欧盟指导文件：食品和饲料中农药残留分析的质量控制和验证程序 The LOQs for the pesticides were determined based on the recovery and RSD results, and defined as the selected lowest validated spike level meeting the requirement of recovery and RSD for different fortification levels, as described in Document No. Quality Control of Pesticides Products. We work to build a strong European Health Union, to improve public health and boost health preparedness and resilience in our Union. 40%) and within-laboratory reproducibility (6. SANCO/12495/2011 (2011 EURL Joint Workshop, Germany) 8. SANCO/12571/ Introduction The guidance in this document is intended for laboratories involved in official control of pesticide residues in food and feed in the European Union. 5 μg kg −1) and quantification (5. a AQC-Guidelines or AQC-Procedures) (SANCO/12574/2014 rev. 12571/2013. 1 16/11/2010 Dec 19, 2014 · The method was based on ultra performance liquid chromatography–quadrupole-time of flight–mass spectrometry (UPLC–QTOF–MS). The document describes the method validation and analytical quality control (AQC) requirements to support the validity of data used for checking compliance with maximum residue limits (MRLs), enforcement actions, or assessment of consumer exposure to pesticides1. 28–10. Für die Genehmigung der Wirkstoffe für Pflanzenschutzmittel und die Zulassung von Pflanzenschutzmitteln hat der Gesetzgeber verbindlich vor-gegeben, nach welchen Testrichtlinien (Guidelines) die entsprechenden Untersuchungen durchzuführen sind. SANTE/1 1945/2015 (2015 EURL Joint Workshop, Germany) We would like to show you a description here but the site won’t allow us. Mar 1, 2019 · The validated method satisfied linearity, sensitivity and recovery, as specified in SANCO No. It establishes criteria for sampling, sample analysis including extraction, clean-up, chromatography, calibration, and quality control. The whole analytical method demonstrated to be quick, simple and reproducible. Guidance Document on Pesticide Analytical Methods for Risk Assessment and Post-approval Control and Monitoring Purposes1 Supersedes Guidance Documents SANCO/3029/99 and SANCO/825/00 The standard ISO/ IEC 17025 and the European technical guidance SANCO/ 12571/2013 on Method Validation and Quality Procedures for Pesticide Residues in Food and Feed requires to test the stability of standard solutions (European Standard 2005; Directorate General for Health and Consumer Affairs (DG SANCO) 2013). Recoveries in the fortification range of 1–40 μg/kg were within 70–120% with associated relative standard deviations below 20% for most of the compounds. According to document No. Main changes introduced into the revision of Document No SANCO/12495/2011 during the Updating Session held in Almeria, October 2013 Global reorganisation of the document structure (changing the order of many paragraphs). Introduction 1. Appendix F: Guidelines for standard method performance requirements ENFSI Standing Committee (QCC-VAL-001, 2006) CEN, (EN 15662:2008) AGENDA ITEM 9 PROPOSED DRAFT GUIDELINES ON PERFORMANCE CRITERIA SPECIFIC FOR Oct 5, 2015 · The method finally proposed (extraction with acetonitrile and a subsequent 2-fold dilution with water without any clean-up step) was fully validated at 0. 010 mg/kg (limit of quantification). 1–118. The document describes the method validation and analytical quality control (AQC) requirements to support the validity of data used for checking compliance with maximum residue limits (MRLs), enforcement This document is revised each year following the Working Group (WG) Meeting of Experts on monitoring of pesticide residues in/on food. Sep 1, 2015 · Document SANCO/12571/2013. DRAFT SANCO/2012/11251 rev. 3% and 12. 0 Guidance document on analytical quality control and validation procedures for pesticide residues analysis in food and feed. The LOQs for the 213 pesticides ranged between 2 and 10 μg/kg. 5–2. 70%), limits of detection (1. 5 22 March 2019 Guidance Document on the renewal of approval of active substances to be assessed in compliance with Regulation (EU) No 844/2012 DG SANCO should reduce the number of priority areas in the annual work plans by allowing a maximum of five priority areas in each of the three strands to increase the impact within the priority areas, bringing them to not more than 15 per yearly call.

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